PTFE BEC 50 mL - PTFE Basic Electrochemical Cell

This cell is a sister version of the BEC 50 mL. In this cell concept, all elements that stay in contact with an electrolyte or its fumes are made of PTFE and other fluorinated materials (tubing, fittings, and O-Rings). This cell is used wherever PEEK fails, i.e. when using electrolytes containing: Aqua regia, Benzenesulfonic acid, Bromine (liquid), Carbolic Acid (Phenol), Carbon Disulfide, Chlorine (aqueous and anhydrous liquid), Chlorosulfonic acid, Chromic Acid, Ethylene bromide (anhydrous), Fuming sulphuric acid (Oleum), Hydrobromic acid, Hydrofluoric acid, Nitric acid (>50%), Sulphuric acid (concentrated 96%), Sulphurous acid. The chamber is also alkali-resistant, so it can be used instead of glass in experiments including high pH hot electrolytes.

This is a stationary solution basic electrochemical (electrolytic) cell for measurements of electrodes in a form of: a) rod/disc (6 mm dia.), b) thin film deposited on flat substrate (using a wire clip) and c) membrane (using a wire clip). The working, counter and reference electrodes are mounted in a top casing either in 2-, or 3-electrode setup. When the reference electrode has a glass body, a liquid junction adapter is needed. The cell elements are constructed with materials that are inert to the sample (PTFE). It well fits aqueous (FKM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is gas-tight and can be used when the removal and exclusion of contaminants such as oxygen and water is required by bubbling of an inert gas through the electrolyte.

Application note The reference electrode (or liquid junction adapter insertion tube) tip should be placed at the level of the working electrode center. This will ensure a low potential drop throughout the electrolyte solution for low-current experiments. Various auxiliary electrodes are suitable for this cell including metal wire and metal foil electrodes as well as graphite rod. The bubbling of gas through the solution must be stopped prior to experiment.

Product includes

• 1 x PTFE lid
• 1 x PTFE chamber
• 1 x PTFE plug