
597 Cylindrical FlatSample Cell
AMEL



Small volume test cell for liquid electrolytes with low vapor pressure. Benefit from this test cell for performing electrochemical measurements to study liquid samples with low vapor pressure, e.g. ionic liquids.
This test cell can be used for experiments with both a 2-electrode and a 3-electrode configuration. Typical applications are:
The test cell TSC 70 closed consists of several high-quality building blocks: The gold-plated base unit (= "thermo block") comes with an integrated Pt100 temperature sensor that monitors the temperature very close to the sample, as well as a fixed platinum crucible that serves as sample container and counter electrode. To seal the test cell, a housing made of polyether ether ketone (PEEK) with two o-ring grooves is used which connects the base unit and the cap.
The PEEK cap has an integrated electrode plug made of a soda-lime glass sleeve bearing 4 separately connectable platinum electrodes, each with a polished front-end. Furthermore, the cap has two inlets that are sealed by plugs by default, but can be used for inserting capillaries or (pseudo-) reference electrodes made of metal wires.
Attention: Due to the very low sample volume and the inner dead volume, this test cell is recommended for studying samples with a quite low vapour pressure, e.g. like ionic liquids. For samples with higher vapour pressure, we recommend using the test cell TSC 1600 Closed or TSC 1600 Closed GC instead.
Type
Test Cell
Temperature range
Max. -40 °C to +100 °C
Storage conditions
Storage: +10 °C to +30 °C
Optional accessories
Cap with exchangeable electrode tip
Art. No.
840211
Base unit material
Gold-plated copper with nickel interlayer
Suitable samples
Liquid electrolytes with low vapour pressure, gels with low viscosity
Materials in sample contact
PEEK, Pt, lime soda glass, EPDM, gold
Sample volume
min. 70 µl, max. 100 µl
Diameter Pt electrodes in glass
0.25 mm each
Temperature sensor
Integrated Pt100 temperature sensor
Working electrode material
Platinum
Counter electrode material
Platinum (crucible)
Reference electrode included
Metal-wire based pseudo-reference electrode (as accessory)
Electrode configuration supported
2-electrode and 3-electrode
Air-tight
Yes (inside or outside glovebox
Required accessory for electrical connection
Microcell HC Setup, Microcell Passive, or customized cable set
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